HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 24897854, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Chloroacetyl chloride | HCID 6577 | — |
| Reactant | HCID 57890287 | HCID 57890287 | — |
| Solvent | 1,1-Dichloroethane | HCID 6365 | — |
| Product | HCID 24897854 | HCID 24897854 | 101.9% |
Reaction Steps
Following the procedure of Example 1, 6,7,8,9,10,11-Hexahydro-benzo[b]-cycloocta[d]furan-2-ylamine (0.80 g, 3.7 mmol), chloroacetyl chloride (0.31 mL, 3.9 mmol), and pyridine (0.60 mL, 7.4 mmol) in dichloroethane (25 mL) provided 2-chloro-N-6,7,8,9,10,11-hexahydrobenzo[b]cycloocta[d]furan-2-ylacetamide (1.1 g). MS (ESI) m/z 292 ([M+H]+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07601856B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-13c5267a6a4f49f28c25694bb40f3106 |
| Source note | uspto-grants-2009_10 |