HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → Methyl 4-hydroxy-3-methylbenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | 4-Hydroxy-3-methylbenzoic acid | HCID 68138 | — |
| Product | Methyl 4-hydroxy-3-methylbenzoate | HCID 11240684 | — |
Reaction Steps
To a mixture of 3-methyl-4-hydroxybenzoic acid (342 g, 2.24 mol) in MeOH (3.5 I) is bubbled HCl (g) for 5 m. The mixture is stirred for 12 h at RT. The reaction is concentrated to give the title compound (372 g, quant).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07601850B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-d397260e9acb48b1b6f809ff7490b7b3 |
| Source note | uspto-grants-2009_10 |