Hydrochloric Acid → HCID 69039494, compound

HRID 1820749Notes

Reaction equation

HRID 1820749 reaction equation
[CH3:1][O:2][C:3]([C:5]1[N:6]=[CH:7][C:8]([N:11]2[CH2:16][CH2:15][N:14](C(OC(C)(C)C)=O)[CH2:13][CH2:12]2)=[N:9][CH:10]=1)=[O:4].[ClH:24]>O1CCOCC1>[ClH:24].[CH3:1][O:2][C:3]([C:5]1[N:6]=[CH:7][C:8]([N:11]2[CH2:12][CH2:13][NH:14][CH2:15][CH2:16]2)=[N:9][CH:10]=1)=[O:4]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 52987591HCID 52987591, compound

Product 1

HCID 69039494HCID 69039494, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

Prepared in analogy to example 4.4(b) from 2,3,5,6-Tetrahydro-[1,2′]bipyrazinyl-4,5′-dicarboxylic acid 4-tert-butyl ester 5′-methyl ester and 1,4-dioxane saturated with gaseous HCl. MS (m/e): 223.1 (MH+, 100%)

Sources & evidence

ORD record
ord-b93c56e97c8d4ffaa4fffb71b5450c8a
Source dataset
uspto-grants-2009_10
Patent number
US07605163B2

Reaction notes

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