HuagongsheHuagongshe Chemistry Print Report · For research reference only
Alumina → HCID 57892086, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Alumina | HCID 9989226 | — |
| Reactant | Dichloromethane ethanol | HCID 21584144 | — |
| Reactant | HCID 68980202 | HCID 68980202 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 57892086 | HCID 57892086 | — |
Reaction Steps
Prepared analogously to Example VI.1.d from 1.80 g (7.28 mmol) of 6-nitro-2-(pyrrolidin-1-ylmethyl)benzoxazole (VIII.1.b) in methanol as solvent. Yield: 1.10 g (70% of theory); Rf value: 0.60 (aluminum oxide, dichloromethane/ethanol=20:1); C12H15N3O; EII mass spectrum: m/z=218 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07605176B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-1aa625a669d046d1a2306bdcd6f15e27 |
| Source note | uspto-grants-2009_10 |