HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Dodecanethiol → Sodium dodecane-1-thiolate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Dodecanethiol | HCID 8195 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Sodium dodecane-1-thiolate | HCID 23672953 | — |
Reaction Steps
In another flask, sodium methoxide (1.43 g, 26 mmol) was dissolved in 10 ml methanol, and dodecanethiol (6.5 ml, 27 mmol) was added. The resulting solution was stirred at room temperature for 15 minutes. The solvent was then evaporated under reduced pressure at 90° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07605290B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-9510c937aa0b4a378f0b2a3aa635ced6 |
| Source note | uspto-grants-2009_10 |