HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 68998791, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | HCID 66585324 | HCID 66585324 | — |
| Product | HCID 68998791 | HCID 68998791 | 61% |
Reaction Steps
To Compound 108 (50.0 mg, 0.13 mmol), methanol (1.00 mL) and sulfuric acid (0.07 mL, 1.30 mmol) were added and the mixture was reacted in a microwave reaction vessel at 100° C. for 5 minutes to obtain Compound 121 (31.6 mg, 61%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07605272B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-438d53c3601449ebb4fa364848e83f94 |
| Source note | uspto-grants-2009_10 |