HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 131727673, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | 4-Methylmorpholine | HCID 7972 | — |
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | HCID 131727674 | HCID 131727674 | — |
| Product | HCID 131727673 | HCID 131727673 | — |
Reaction Steps
12 (0.88 g, 2.28 mmol) was treated as described for 13, using CAIBE (2.28 mmol, 0.37 ml), NMM (2.28 mmol, 0.31 ml), diazomethane (14.3 mmol in 15 ml ether) HBr/glacial acetic acid (33%): 4.24 mmol, 1.04 ml.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07608577B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-2fe28f1fd9f94404865fe729f7e594c5 |
| Source note | uspto-grants-2009_10 |