HuagongsheHuagongshe Chemistry Print Report · For research reference only
4,6-dichloro-N-phenyl-1,3,5-triazin-2-amine → HCID 9945961, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4,6-dichloro-N-phenyl-1,3,5-triazin-2-amine | HCID 16766 | — |
| Reactant | 1,3-Benzodioxol-5-amine | HCID 84310 | — |
| Product | HCID 9945961 | HCID 9945961 | 42% |
Reaction Steps
The reaction of 4,6-dichloro-N-phenyl-[1,3,5]triazine-2-amine with 3,4-methylenedioxyaniline using the method described for the synthesis of CT-32028 provided CT-32042 (51 mg, 42% yield). 1H NMR (d6-DMSO) δ 10.05-10.29 (m, 2H), 7.57-7.80 (m, 2H), 7.21-7.42 (m, 3H), 6.80-7.13 (m, 3H), 6.03 (s, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07608620B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-c8591c8a4e4c43de9b65ebdbb94f2f09 |
| Source note | uspto-grants-2009_10 |