HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorophenol → HCID 20561961, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorophenol | HCID 4684 | — |
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | dichlorophosphate | HCID 3718378 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 20561961 | HCID 20561961 | — |
Reaction Steps
3,4-Dichloro-phenyl dichlorophosphate was prepared as described in Example 2 from p-chlorophenol (3.79 g, 0.023 mol), POCl3 (2.17 mL, 0.023 mol) and TEA (3.25 mL, 0.023 mol) and dry Et2O (25 mL).The dichlorophosphate 11c was obtained as a yellow clear oil (2.93 g, 0.0105 mol, 45%) and used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07608599B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-18604279dd4c4550bd0628e0857e566a |
| Source note | uspto-grants-2009_10 |