HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxyphenol → HCID 12585423, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxyphenol | HCID 9015 | — |
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 12585423 | HCID 12585423 | — |
Reaction Steps
p-methoxyphenyl dichlorophosphate (11d) was prepared as described in Example 2 from p-methoxyphenol (4.00 g, 0.032 mol), POCl3 (3.00 mL, 0.032 mol) and TEA (4.49 mL, 0.032 mol) and dry Et2O (25 mL). The dichlorophosphate 11d was obtained as a yellow clear oil (5.1 g, 0.021 mol, 67%) and used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07608599B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-014bc727ed484c92b653119b642bbc52 |
| Source note | uspto-grants-2009_10 |