HCID 76852918, compound → HCID 68981209, compound

Participants

Reaction Steps

N-Cyclopentyl-1H-pyrrolo[2,3-c]pyridine-2-carboxamide (20 mg, 43%) was prepared as an off-white solid following the procedure described for Example 27 using 7-chloro-N-cyclopentyl-1H-pyrrolo[2,3-c]pyridine-2-carboxamide and ethanol as a solvent: mp 220-224° C.; 1H NMR (300 MHz, CD3OD) δ1.22-2.18 (8H, m), 4.28-4.42 (1H, m), 7.27 (1H, s), 7-82 (1H, d, J=5.8 Hz), 8.15 (1H, d, J=5.8 Hz), 8.85 (1H, s); ESI MS m/z 230 [C13H15N3O+H]+; HPLC (Method A) >99% (AUC), tR=12.1 min.

Provenance & Evidence