HCID 57893442, compound → HCID 57893527, compound

Participants

Reaction Steps

(4-Methoxyphenyl)(1H-pyrrolo[2,3-c]pyridin-2-yl)methanone (87 mg, 99%) was prepared as an off-white solid following the procedure described for Example 100 using (4-methoxyphenyl)(1H-pyrrolo[2,3-c]pyridin-2-yl)methanol (Example 99) and tetrahydrofuran as a solvent: mp 225-228° C.; 1H NMR (300 MHz, CD3OD) δ3.92 (3H, s), 7.10-7.19 (3H, m), 7.75-7.76 (1H, m), 8.02-8.06 (2H, m), 8.16 (1H, d, J=5.6 Hz), 8.86 (1H, s); ESI MS m/z 253 [C15H12N2O2+H]+; HPLC (Method A) >99% (AUC), tR=15.3 min.

Provenance & Evidence