HCID 57893523, compound → HCID 57893485, compound

Participants

Reaction Steps

(4-Chlorophenyl)(1H-pyrrolo[2,3-c]pyridin-2-yl)methanone (108 mg, 67%) was prepared as a yellow solid following the procedure described for Example 100 using (4-chlorophenyl)(1H-pyrrolo[2,3-c]pyridin-2-yl)methanol (Example 101) and tetrahydrofuran as a solvent: mp 274-277° C. dec.; 1H NMR (300 MHz, CD3OD) δ7.21 (1H, s), 7.60-7.63 (2H, m), 7.73-7.76 (1H, m), 7.99-8.03 (2H, m), 8.16 (1H, d, J=5.6 Hz), 8.88 (1H, s); ESI MS m/z 257 [C14H9ClN2O+H]+; HPLC (Method A) >99% (AUC), tR=16.3 min.

Provenance & Evidence