O-Methylhydroxylamine hydrochloride → HCID 136386512, compound

HRID 1821896Notes

Reaction equation

HRID 1821896 reaction equation
[C:1]1([C:7]([C:9]2[NH:17][C:12]3=[CH:13][N:14]=[CH:15][CH:16]=[C:11]3[CH:10]=2)=O)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[ClH:18].[CH3:19][O:20][NH2:21]>>[ClH:18].[CH3:19][O:20][N:21]=[C:7]([C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)[C:9]1[NH:17][C:12]2=[CH:13][N:14]=[CH:15][CH:16]=[C:11]2[CH:10]=1

Participants

3

Reactant 2

HCID 521874O-Methylhydroxylamine hydrochlorideHCID 57893467HCID 57893467, compound

Product 1

HCID 136386512HCID 136386512, compound

Procedure

Phenyl (1H-pyrrolo[2,3-c]pyridin-2-yl)methanone O-methyloxime hydrochloride was prepared from phenyl(1H-pyrrolo[2,3-c]pyridin-2-yl)methanone (Example 35) and O-methylhydroxylamine hydrochloride following the procedure described for Example 104 (geometry of the oxime double bond undefined).

Sources & evidence

ORD record
ord-59731ebaacd642b08da3bf580f8daccb
Source dataset
uspto-grants-2009_10
Patent number
US07608627B2

Reaction notes

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