Potassium Iodide → HCID 86602301, compound

Participants

Reaction Steps

900 mg of 3,5-dichloro-4-{3-[4-(5-isopropylsulfanyl-tetrazol-1-yl)-phenoxy]-propoxy}-phenol, 720 mg of 1,1,1,3-tetrachloropropane, 691 mg of potassium carbonate and 10 mg of potassium iodide are stirred for 48 hours at 60° C. in 30 ml of acetone. The reaction mixture is filtered and the filtrate is concentrated. Purification over silica gel yields the title compound (compound 1.20).

Provenance & Evidence