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HRID1822267

反应详情

EQUATION

反应方程式

HRID 1822267 的结构方程式

REACTANTS

反应物

2
结构：Oc1ccc(Cl)cc1Oc1ccccc1
HCID12774295

4-Chloro-2-phenoxyphenol

C12H9ClO2

结构：COC(=O)CCc1ccc(Oc2cc(F)cc(Br)c2)cc1C
HCID57894233

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc(Oc2cc(F)cc(Oc3ccc(Cl)cc3Oc3ccccc3)c2)ccc1CCC(=O)O
HCID11283285

未命名化合物

PROCEDURE

实验过程

The title compound is prepared by reacting the compound of 3-[4-(3-bromo-5-fluoro-phenoxy)-2-methyl-phenyl]-propionic acid methyl ester with 4-chloro-2-phenoxy-phenol as in Example 18 to afford 0.118 g (22%). 1H NMR (400 MHz, CDCl3); MS (ES+) m/z mass calculated for C28H22O5ClF 492, found 493 and 495 (M+1 and M+3).

WORKUP

后处理

  1. customto afford 0.118 g (22%)