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HRID1822279

反应详情

EQUATION

反应方程式

HRID 1822279 的结构方程式

REACTANTS

反应物

2
结构：Oc1ccc(Cl)cc1Oc1ccccc1
HCID12774295

4-Chloro-2-phenoxyphenol

C12H9ClO2

结构：COC(=O)CCc1ccc(Oc2cc(C)cc(Br)c2)cc1C
HCID57894212

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc(Oc2ccc(CCC(=O)O)c(C)c2)cc(Oc2ccc(Cl)cc2Oc2ccccc2)c1
HCID11477347

未命名化合物

PROCEDURE

实验过程

The title compound is prepared by reacting the compound of 3-[4-(3-bromo-5-methyl-phenoxy)-2-methyl-phenyl]-propionic acid methyl ester with 4-chloro-2-phenoxy-phenol as in Example 18 to afford 0.118 g (22%). 1H NMR (400 MHz, CDCl3); HRMS (ES+) m/z exact mass calculated for C29H25O5Cl 489.1469, found 489.1457.

WORKUP

后处理

  1. customto afford 0.118 g (22%)