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HRID1822306

反应详情

EQUATION

反应方程式

HRID 1822306 的结构方程式

REACTANTS

反应物

2
结构：CCC[CH2][Sn]([CH2]CCC)([CH2]CCC)[c]1ccccn1
HCID607784

2-(Tributylstannyl)pyridine

C17H31NSn

结构：CCOC(=O)CCc1ccc(Oc2cc(F)cc(Oc3ccc(C(F)(F)F)cc3Br)c2)cc1C
HCID57894125

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc(Oc2cc(F)cc(Oc3ccc(C(F)(F)F)cc3-c3ccccn3)c2)ccc1CCC(=O)O
HCID11237570

未命名化合物

PROCEDURE

实验过程

The title compound is prepare by reacting the compound of 3-{4-[3-(2-bromo-4-trifluoromethyl-phenoxy)-5-fluoro-phenoxy]-2-methyl-phenyl}-propionic acid ethyl ester with 2-tributylstannyl pyridine as in Example 39 to afford 0.085 g (36%). 1H NMR (400 MHz, CDCl3); HRMS (ES+) m/z exact mass calculated for C28H21NO4F4 512.1485, found 512.1487.

WORKUP

后处理

  1. customto afford 0.085 g (36%)