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HRID1822320

反应详情

EQUATION

反应方程式

HRID 1822320 的结构方程式

REACTANTS

反应物

2
结构：Oc1ccc(Cl)cc1Oc1ccccc1
HCID12774295

4-Chloro-2-phenoxyphenol

C12H9ClO2

结构：COC(=O)CCc1ccc(Oc2cccc(Br)c2C)cc1C
HCID57894138

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc(Oc2cccc(Oc3ccc(Cl)cc3Oc3ccccc3)c2C)ccc1CCC(=O)O
HCID57894157

未命名化合物

收率 9%

PROCEDURE

实验过程

3-[4-(3-bromo-2-methyl-phenoxy)-2-methyl-phenyl]-propionic acid methyl ester is reacted with 4-chloro-2-phenoxy-phenol as in Example 18 to afford 0.031 g (9%) of the title compound. 1H NMR (400 MHz, CDCl3); MS (ES+) m/z mass calculated for C29H25O5Cl 488, found 489 and 491 (M+1 and M+3, 100%).