HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloro-2-phenoxyphenol → 3-{4-[3-(4-Chloro-2-phenoxy-phenoxy)-2-methyl-phenoxy]-2-methyl-phenyl}-propionic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloro-2-phenoxyphenol | HCID 12774295 | — |
| Reactant | 3-[4-(3-Bromo-2-methyl-phenoxy)-2-methyl-phenyl]-propionic acid methyl ester | HCID 57894138 | — |
| Product | 3-{4-[3-(4-Chloro-2-phenoxy-phenoxy)-2-methyl-phenoxy]-2-methyl-phenyl}-propionic acid | HCID 57894157 | 9% |
Reaction Steps
3-[4-(3-bromo-2-methyl-phenoxy)-2-methyl-phenyl]-propionic acid methyl ester is reacted with 4-chloro-2-phenoxy-phenol as in Example 18 to afford 0.031 g (9%) of the title compound. 1H NMR (400 MHz, CDCl3); MS (ES+) m/z mass calculated for C29H25O5Cl 488, found 489 and 491 (M+1 and M+3, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07608639B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-d2bdfe71ff634116a14c8e67ff470314 |
| Source note | uspto-grants-2009_10 |