HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68489029, compound → HCID 68491417, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68489029 | HCID 68489029 | — |
| Solvent | Trifluoroacetic acid methylene chloride | HCID 21863450 | — |
| Product | HCID 68491417 | HCID 68491417 | — |
Reaction Steps
Compound 20 was kept in dichloromethane-trifluoroacetic acid 2:1 for 1 h at rt and concentrated to dryness. The residue was dried in a vacuum for 16 hrs. Reversed phase C18 HPLC showed >95% purity M+H+283.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07608590B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-12b96bb212384a99b53aff70d0acaa1b |
| Source note | uspto-grants-2009_10 |