HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 68493037, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | HCID 68491072 | HCID 68491072 | — |
| Solvent | Trifluoroacetic acid methylene chloride | HCID 21863450 | — |
| Product | HCID 68493037 | HCID 68493037 | 100% |
Reaction Steps
Compound 72 was kept in DCM-TFA 2:1 (2 mL) for 2.5 hr at RT. The solution was co-evaporated with toluene to dryness. Yield 100%. M+H 603.12
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07608590B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-5836c00abf8048eaa0d6d195da855186 |
| Source note | uspto-grants-2009_10 |