Diethanolamine → HCID 312172, compound

HRID 1822652Notes

Reaction equation

HRID 1822652 reaction equation
[F:1][C:2]([F:13])([F:12])[C:3]1[CH:4]=[C:5]([B:9]([OH:11])[OH:10])[CH:6]=[CH:7][CH:8]=1.[NH:14]([CH2:18][CH2:19]O)[CH2:15][CH2:16]O>>[F:13][C:2]([F:1])([F:12])[C:3]1[CH:4]=[C:5]([B:9]2[O:10][CH2:19][CH2:18][NH:14][CH2:15][CH2:16][O:11]2)[CH:6]=[CH:7][CH:8]=1

Participants

3

Reactant 2

HCID 8113DiethanolamineHCID 27343883-(Trifluoromethyl)phenylboronic acid

Product 1

HCID 312172HCID 312172, compoundYield 79%

Procedure

The title compound (79%, crystals) was prepared from 3-trifluoromethylphenylboronic acid and diethanolamin.

Sources & evidence

ORD record
ord-5293990da7be4759a387a29bdf36f0ab
Source dataset
uspto-grants-2006_05
Patent number
US07037905B2

Reaction notes

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