Diethanolamine → HCID 10399596, compound

HRID 1822653Notes

Reaction equation

[F:1][C:2]1[CH:3]=[C:4]([B:10]([OH:12])[OH:11])[CH:5]=[C:6]([F:9])[C:7]=1[F:8].[NH:13]([CH2:17][CH2:18]O)[CH2:14][CH2:15]O>>[F:1][C:2]1[CH:3]=[C:4]([B:10]2[O:11][CH2:18][CH2:17][NH:13][CH2:14][CH2:15][O:12]2)[CH:5]=[C:6]([F:9])[C:7]=1[F:8]

Participants

Reactant 2

HCID 8113Diethanolamine

HCID 2734671(3,4,5-Trifluorophenyl)boronic Acid (contains varying amounts of Anhydride)

Product 1

HCID 10399596HCID 10399596, compoundYield 70%

Procedure

The title compound (70%, crystals) was prepared from 3,4,5-trifluorophenylboronic acid and diethanolamin.

Sources & evidence

ORD record: ord-d565f40f881b4dda85c09b8e12d64366
Source dataset: uspto-grants-2006_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07037905B2

Reaction notes

Loading…