Diethanolamine → HCID 22169590, compound

HRID 1822658Notes

Reaction equation

HRID 1822658 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([B:9]([OH:11])[OH:10])[CH:5]=[C:6]([Cl:8])[CH:7]=1.[NH:12]([CH2:16][CH2:17]O)[CH2:13][CH2:14]O>>[Cl:8][C:6]1[CH:5]=[C:4]([B:9]2[O:10][CH2:17][CH2:16][NH:12][CH2:13][CH2:14][O:11]2)[CH:3]=[C:2]([Cl:1])[CH:7]=1

Participants

3

Reactant 2

HCID 8113DiethanolamineHCID 27343313,5-Dichlorophenylboronic acid

Product 1

HCID 22169590HCID 22169590, compoundYield 94%

Procedure

The title compound (94%, crystals) was prepared from 3,5-dichlorophenylboronic acid and diethanolamin.

Sources & evidence

ORD record
ord-bc5af60413a24c36b2e01e55abc00783
Source dataset
uspto-grants-2006_05
Patent number
US07037905B2

Reaction notes

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