HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 23568572, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | HCID 16493899 | HCID 16493899 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 23568572 | HCID 23568572 | — |
Reaction Steps
N-Boc-L-leucine 3-methoxypropyl amide (463 mg, 1.54 mmol) was in CH3OH (10 mL) was treated with acetyl chloride (1 mL). After 45 minutes, all volatiles were removed under reduced pressure to yield L-leucine 3-methoxypropyl amide hydrochloride (310 mg, quant.) as a sticky solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07037916B2 |
| Source dataset | uspto-grants-2006_05 |
| ORD ID | ord-1d9f200111214a378dce22ad4b94c051 |
| Source note | uspto-grants-2006_05 |