HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 1-(3-chloropropyl)-1H-1,2,4-triazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 3-(1H-1,2,4-triazol-1-yl)propan-1-ol | HCID 4711802 | — |
| Product | 1-(3-chloropropyl)-1H-1,2,4-triazole | HCID 16790688 | — |
Reaction Steps
3-(1H-1,2,4-triazol-1-yl)-1-propanol (0.160 g, 1.3 mmol) was refluxed in thionylchloride (3 ml) for 2 h. The recation mixture was evaporated yielding the title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07037925B2 |
| Source dataset | uspto-grants-2006_05 |
| ORD ID | ord-b173af9441ee4641b250be0b825fc624 |
| Source note | uspto-grants-2006_05 |