HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14801183, compound → 39053-19-5
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14801183 | HCID 14801183 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol ethylacetate | HCID 21584252 | — |
| Product | 39053-19-5 | HCID 14801184 | 78.7% |
Reaction Steps
A mixture of methyl 2-methyl-3-nitrobenzyl ether (0.19 g, 1.05 mmol), and 5% Pd/C (70 mg) in EtOAc/EtOH 1:1 (14 ml) was hydrogenated at 1 atm over night. The mixture was filtered through Celite, and the filtrate was concentrated to give the title compound 125 mg (78%) as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07037925B2 |
| Source dataset | uspto-grants-2006_05 |
| ORD ID | ord-0a1c6ec283e84342b376c613275e3f38 |
| Source note | uspto-grants-2006_05 |