Phenol → HCID 178461642, compound

Participants

Reaction Conditions

Reaction Steps

In the drybox, a 100-mL Schlenk flask was charged with Et2O (30 mL) and cooled to −78° C. Diethylzinc (9.0 mL of a 1.0 M hexane solution, 9.0 mmol) was added via syringe. A solution of phenol (0.847 g of phenol in 10 mL of Et2O) was added to the Schlenk flask, and the colorless reaction mixture was stirred at −78° C. for 1 h. The mixture was evaporated to give a white solid (1.593 g, 94%). 1H NMR (300 MHz, DMSO-d6): δ 7.1, 6.6 (m, 5H), 1.2 (t, 3H), 0.1 (m, 2H).

Provenance & Evidence