HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromofuran-2-carboxylic acid → HCID 9901891, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromofuran-2-carboxylic acid | HCID 605479 | — |
| Reactant | HCID 136279893 | HCID 136279893 | — |
| Product | HCID 9901891 | HCID 9901891 | — |
Reaction Steps
The title compound was prepared from 3-bromo-furan-2-carboxylic acid (381.7 mg, 2.00 mmol) and 5-chloro-pyridine-2-amidoxime (343 mg, 2.00 mmol), similar to Example 70, and yielded 353 mg (54%) of white solid. 1H NMR (CDCl3): 8.81 (d, J=2.47 Hz, 1H), 8.22 (d, J=8.24 Hz, 1H), 7.90 (dd, J=8.25, 2.48 Hz, 1H), 7.71 (d, J=1.93 Hz, 1H), 6.79 (d, J=1.64 Hz, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07041685B2 |
| Source dataset | uspto-grants-2006_05 |
| ORD ID | ord-2d61159cc5174d7291661c2c259c21a0 |
| Source note | uspto-grants-2006_05 |