HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chlorothiophene-2-carbonyl chloride → HCID 22147858, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chlorothiophene-2-carbonyl chloride | HCID 2735824 | — |
| Reactant | HCID 2744266 | HCID 2744266 | — |
| Product | HCID 22147858 | HCID 22147858 | — |
Reaction Steps
The title compound was prepared from 2-methyl-thiazole-4-amidoxime (24.6 mg, 0.156 mmol) and 3-chloro-thiophene-2-carbonyl chloride (28.7 mg, 0.159 mmol) similar to Example 16, and yielded 18.2 mg (40%) of white solid. 1H NMR (CDCl3): 8.03 (s, 1H), 7.61 (d, J=5.49 Hz, 1H), 7.13 (d, J=5.22 Hz, 1H), 2.84 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07041685B2 |
| Source dataset | uspto-grants-2006_05 |
| ORD ID | ord-f6861d2e74394ce88b60ae33371ffc9e |
| Source note | uspto-grants-2006_05 |