3-Chlorothiophene-2-carbonyl chloride → HCID 69088651, compound

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The title compound was prepared from 7-methyl-5-trifluoromethyl-pyrazolo[1,5-α]pyrimidine-3-amidoxime (13.8 mg, 0.0532 mmol) and 3-chloro-thiophene-2-carbonyl chloride (9.8 mg, 0.0541 mmol) similar to Example 16, and yielded 9.8 mg (48%) of an off-white solid. 1H NMR (CDCl3): 8.89 (s, 1H), 7.62 (d, J=5.22 Hz, 1H), 7.20 (d, J=0.83 Hz, 1H), 7.14 (d, J=5.22 Hz, 1H), 2.98 (s, 3H).

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