Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-(((Tert-butoxy)carbonyl)amino)butanoic acid → methyl N-{2-[(tert-butoxycarbonyl)amino]butanoyl}alaninate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-(((Tert-butoxy)carbonyl)amino)butanoic acid | HCID 333522 | — |
| 반응물 | Methyl 2-aminobutanoate hydrochloride | HCID 13283515 | — |
| 반응물 | methyl{[N-(tert-butoxycarbonyl)-L-alanyl]amino}(cyclopropyl)acetate | HCID 58583288 | — |
| 생성물 | methyl N-{2-[(tert-butoxycarbonyl)amino]butanoyl}alaninate | HCID 86588879 | — |
반응 단계
Following the procedure for the preparation of methyl{[N-(tert-butoxycarbonyl)-L-alanyl]amino}(cyclopropyl)acetate but substituting N-Boc-alpha-aminobutyric acid and methyl 2-aminobutanoate hydrochloride and making non-critical variations provided the title compound as a solid: 1H NMR (CDCl3) δ 0.82–0.91, 1.24–1.38, 1.52, 1.68–2.05, 3.75, 4.20, 4.52–4.59, 5.05, 6.69.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07041672B2 |
| 출처 데이터셋 | uspto-grants-2006_05 |
| ORD ID | ord-ebc1d4e1101743fa9cb61b75551fb7f9 |
| 출처 메모 | uspto-grants-2006_05 |