HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl({2-[(tert-butoxycarbonyl)amino]butanoyl}amino)(cyclopropyl)acetate → Methyl[(2-aminobutanoyl)amino](cyclopropyl)acetate hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl({2-[(tert-butoxycarbonyl)amino]butanoyl}amino)(cyclopropyl)acetate | HCID 23593721 | — |
| Reactant | methyl(L-alanylamino)(cyclopropyl)acetate hydrochloride | HCID 86588880 | — |
| Product | Methyl[(2-aminobutanoyl)amino](cyclopropyl)acetate hydrochloride | HCID 86588881 | — |
Reaction Steps
Following the procedure for the preparation of methyl(L-alanylamino)(cyclopropyl)acetate hydrochloride but substituting methyl({2-[(tert-butoxycarbonyl)amino]butanoyl}amino)(cyclopropyl)acetate and making non-critical variations provided the title compound as a solid: 1H NMR (DMSO-d6) δ 0.29–0.40, 0.88–0.94, 1.12, 1.37, 1.75–1.82, 3.57, 3.62–3.79, 8.29.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07041672B2 |
| Source dataset | uspto-grants-2006_05 |
| ORD ID | ord-b9d63075769048ae8ebbbb4233055ec8 |
| Source note | uspto-grants-2006_05 |