Propylamine → HCID 178456948, compound

HRID 1824455Notes

Reaction equation

HRID 1824455 reaction equation
[Cl:1][C:2]1[N:10]=[C:9]2[C:5]([NH:6][CH:7]=[N:8]2)=[C:4](Cl)[N:3]=1.[CH2:12]([NH2:15])[CH2:13][CH3:14]>C(O)CCC>[CH2:12]([NH:15][C:4]1[NH:3][C:2]([Cl:1])=[N:10][C:9]2[C:5]=1[N:6]=[CH:7][N:8]=2)[CH2:13][CH3:14]

Participants

4

Reactant 2

HCID 7852PropylamineHCID 53244122,6-Dichloropurine

Product 1

HCID 178456948HCID 178456948, compound

Reagents, catalysts & solvents 1

HCID 2631-ButanolSolvent

Conditions

Temperature
75 °C

Procedure

189 mg of 2,6-dichloropurine, 4 ml of butanol and 0.09 ml (1.1 mol) of propylamine are mixed at room temperature and the medium is heated at a temperature of 75° C. for 2 hours 30 minutes.

Sources & evidence

ORD record
ord-0c5e4be440cc4f2bb9f0e8dba01e17f2
Source dataset
uspto-grants-2006_05
Patent number
US07041824B2

Reaction notes

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