참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | HCID 178505790 | HCID 178505790 | — |
| 반응물 | HCID 178511674 | HCID 178511674 | — |
| 생성물 | HCID 178511654 | HCID 178511654 | — |
반응 단계
570 mg of trans-1,4-diaminocyclohexane are heated to its melting point 70° C., 290 mg of the product obtained in stage 1 above are added and the medium is then heated at approximately 140° C. for about 4 hours and then left overnight at room temperature. After purification by chromatography on silica with, as eluent, a mixture of CH2Cl2:MeOH:NH4OH (75:22:3) 93 mg of the expected product are obtained in the form of a beige crumbly foam.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07041824B2 |
|---|
| 출처 데이터셋 | uspto-grants-2006_05 |
|---|
| ORD ID | ord-6161ce87d47a422ba0ebfecb3612d3e3 |
|---|
| 출처 메모 | uspto-grants-2006_05 |
|---|
