HCID 22142146, compound → HCID 67457713, compound

Participants

Reaction Steps

To the product (0.42 g) of Step 4 of Example 1 was added dichloromethane (10 mL) and 5% aqueous sodium hypochlorite (20 mL). The two-phase mixture was stirred vigorously overnight at room temperature, the organic layer was separated, dried over anhydrous sodium sulfate, and concentrated under reduced pressure to give a red oil (0.4 g).

Provenance & Evidence