HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromo-4-fluorophenyl acetate → 3-Bromo-4-Fluorophenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromo-4-fluorophenyl acetate | HCID 20785459 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Diisopropylethylamine | HCID 81531 | — |
| Product | 3-Bromo-4-Fluorophenol | HCID 2783381 | — |
Reaction Steps
A solution of 0.80 gm (3.43 mMol) O-acetyl 3-bromo-4-fluorophenol in 10 mL 6% diisopropylethylamine in methanol was stirred at room temperature for 8 hours. The reaction mixture was concentrated under reduced pressure at 0° C. to provide the desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07045545B1 |
| Source dataset | uspto-grants-2006_05 |
| ORD ID | ord-cf7bf73dee2b4db091aec6dda1a71648 |
| Source note | uspto-grants-2006_05 |