HRID1824935

反应详情

EQUATION

反应方程式

HRID 1824935 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A solution of 0.80 gm (3.43 mMol) O-acetyl 3-bromo-4-fluorophenol in 10 mL 6% diisopropylethylamine in methanol was stirred at room temperature for 8 hours. The reaction mixture was concentrated under reduced pressure at 0° C. to provide the desired compound.

WORKUP

后处理

  1. concentrationThe reaction mixture was concentrated under reduced pressure at 0° C.