HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 286836-32-6
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | 5-(2-Aminopropyl)benzofuran | HCID 9837232 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 286836-32-6 | HCID 22144718 | 91% |
Reaction Steps
This amine was dissolved in 20 mL ethyl acetate and then a 1 N solution of hydrogen chloride in diethyl ether was added dropwise. The resulting slurry was filtered, the solid washed with 3 mL ethyl acetate, and the solid dried under vacuum to provide 0.548 gm (91%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07045545B1 |
| Source dataset | uspto-grants-2006_05 |
| ORD ID | ord-33537da81d28443381d818022afc5fe4 |
| Source note | uspto-grants-2006_05 |