Morpholine → HCID 22139428, compound

Participants

Reaction Steps

Morpholine (0.96 ml, 11 mmol) was added to a solution of 3-oxo-3-thianthren-1-yl-dithiopropionic acid ethyl ester (3.99 g, 11 mmol) in ethanol (20 ml). The reaction was refluxed for 8 hours and was then cooled to room temperature. The precipitate formed was filtered and dried to give the desired product as a bright orange solid (3.50 g, 82%). m/z (LC-MS, ESP), RT=4.81 and 5.33 min same (M+1)=388

Provenance & Evidence