4,5-Dichloro-1,2-phenylenediamine → HCID 131725761, compound

Participants

Reaction Steps

N-(2-Amino-4,5-dichlorophenyl)-N′-(4-methyl-3-thienyl)thiourea is obtained analogously to the reaction described in example 1b) from 4-methyl-3-thienyl isothiocyanate and 4,5-dichloro-1,2-diaminobenzene. Crystalline solid, m.p. 310-320° C. b) 3N-(5,6-Dichloro-2-benzimidazolyl)-4-methyl-3-thienylamine hydrochloride is obtained analogously to the procedure described in example 1c) from N-(2-amino-4,5-dichlorophenyl)-N′-(4-methyl-3-thienyl)thiourea and methyl iodide.

Provenance & Evidence