HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53794133, compound → HCID 11746630, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53794133 | HCID 53794133 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 11746630 | HCID 11746630 | 100.5% |
Reaction Steps
Ethyl 2-ethyl-3-(4-methoxyphenyl)acrylate (4.58 g, 19.5 mmol), 5% palladium on carbon (500 mg) and ethyl acetate (100 mL) were mixed and hydrogenated for 8 hours at room temperature. After the catalyst was removed by filtration, the filtrate was concentrated to afford 4.63 g (100%) of the title compound as a pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07049342B2 |
| Source dataset | uspto-grants-2006_05 |
| ORD ID | ord-824807bc8a6846c58bbfc67e1e4f0688 |
| Source note | uspto-grants-2006_05 |