HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22139632, compound → HCID 22139631, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22139632 | HCID 22139632 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 22139631 | HCID 22139631 | — |
Reaction Steps
To a stirring solution of 3-methyl-2-(1-methyl-piperidin-4-yl)-5-nitro-6-pyridin-4-yl-3H-pyrimidin-4-one (0.34 mmol) in methanol was added Pd/C (20 mg) and the reaction was stirred overnight under a hydrogen filled balloon. The reaction was filtered through celite then the product was purified on silica. M+1=299.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07049318B2 |
| Source dataset | uspto-grants-2006_05 |
| ORD ID | ord-3c7bda66b97d4f1f84ead9b25d838d2f |
| Source note | uspto-grants-2006_05 |