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HRID1826600

反应详情

EQUATION

反应方程式

HRID 1826600 的结构方程式

REACTANTS

反应物

1
结构：COc1ccc(C(=O)N[C@@H](CN=[N+]=[N-])c2ccccc2)cc1
HCID53998160

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc(C(=O)N[C@@H](CN)c2ccccc2)cc1
HCID54421380

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

Using Deprotection Method A, (R)-2-(4-methoxybenzoylamino)-2-phenylethyl azide (46.3 g) in THF (400 mL) afforded, after recrystallization with ethyl acetate, 35.4 g (84%) of the title compound.

WORKUP

后处理

  1. customafforded
  2. customafter recrystallization with ethyl acetate, 35.4 g (84%) of the title compound