HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methylcyclohexylamine, mixed isomers → N-(3-Methylcyclohexyl)-2-quinoxalinecarboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methylcyclohexylamine, mixed isomers | HCID 110931 | — |
| Reactant | Quinoxaline-2-carbonyl chloride | HCID 2734681 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | N-(3-Methylcyclohexyl)-2-quinoxalinecarboxamide | HCID 22136416 | 78.4% |
Reaction Steps
Prepared from 2-quinoxaloyl chloride (193 mg, 1.0 mmol), 3-methylcyclohexylamine (119 mg, 0.90 mmol), and pyridine (5 mL) yielding 190 mg (78%) of (161):
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07053104B2 |
| Source dataset | uspto-grants-2006_05 |
| ORD ID | ord-0d22c7f232e6468d936e11142047278a |
| Source note | uspto-grants-2006_05 |