HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dimethylcyclohexylamine → HCID 22136401, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dimethylcyclohexylamine | HCID 123507 | — |
| Reactant | Quinoxaline-2-carbonyl chloride | HCID 2734681 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 22136401 | HCID 22136401 | 59% |
Reaction Steps
Prepared from 2-quinoxaloyl chloride (193 mg, 1.0 mmol), 2,3-dimethylcyclohexylamine (115 mg, 0.90 mmol), and pyridine (5 mL) yielding 150 mg (59%) of (163): rt=10.12 min.; m/z (rel. int.) 283 (M+, 35), 212 (6), 198 (14), 175 (6), 174 (39), 158 (7), 157 (22), 131 (6), 130 (46), 129 (100), 126 (44), 109 (8), 103 (20), 103 (20), 102 (45), 76 (13), 75 (11), 67 (7), 56 (10), 55 (12), 51 (6), 43 (6), 41 (16).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07053104B2 |
| Source dataset | uspto-grants-2006_05 |
| ORD ID | ord-4e85c1aa695944f0b9d4e0c6f900bffc |
| Source note | uspto-grants-2006_05 |