HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-4-aminopyrimidine → HCID 23577296, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-4-aminopyrimidine | HCID 345752 | — |
| Reactant | [1-(2-Phenylethylsulfonyl)piperidin-4-yl]methanamine | HCID 22135729 | — |
| Product | HCID 23577296 | HCID 23577296 | — |
Reaction Steps
EXAMPLE 96 was prepared from C-[1-(2-phenyl-ethanesulfonyl)-piperidin-4-yl]-methylamine and 2-chloro-pyrimidin-4-ylamine (prepared from 2,4-chloro-pyrimidin-4-ylamine by hydrogenation in ethanol over 5% palladium on carbon, 1 atm of hydrogen): MS (m+1)=376.5.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07053089B2 |
| Source dataset | uspto-grants-2006_05 |
| ORD ID | ord-c8717dbc633e419a979d28abced4d5db |
| Source note | uspto-grants-2006_05 |