4-Nitrophenol → HCID 22137959, compound

HRID 1827401Notes

Reaction equation

[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([OH:10])=[CH:6][CH:5]=1)([O-:3])=[O:2].[F:11][C:12]1[CH:19]=[C:18]([F:20])[C:17]([F:21])=[CH:16][C:13]=1[CH2:14]Br>>[F:21][C:17]1[CH:16]=[C:13]([CH2:14][O:10][C:7]2[CH:8]=[CH:9][C:4]([N+:1]([O-:3])=[O:2])=[CH:5][CH:6]=2)[C:12]([F:11])=[CH:19][C:18]=1[F:20]

Participants

Reactant 2

HCID 9804-Nitrophenol

HCID 27770572,4,5-Trifluorobenzyl Bromide

Product 1

HCID 22137959HCID 22137959, compoundYield 92%

Procedure

Prepared in analogy to example 8 from 4-nitrophenol and 2,4,5-trifluoro-benzylbromide. Colorless solid. Yield=92%. MS: m/e=283.0 (M+).

Sources & evidence

ORD record: ord-e9f67473e64f43c9968d1d2725a6e67b
Source dataset: uspto-grants-2006_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07053245B2

Reaction notes

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