Ammonium Hydroxide → HCID 9994024, compound

HRID 1827407Notes

Reaction equation

HRID 1827407 reaction equation
C[O:2][C:3](=O)[CH2:4][C:5]([NH:7][C:8]1[CH:13]=[CH:12][C:11]([O:14][CH2:15][C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)=[CH:10][CH:9]=1)=[O:6].[OH-].[NH4+:24]>>[CH2:15]([O:14][C:11]1[CH:12]=[CH:13][C:8]([NH:7][C:5](=[O:6])[CH2:4][C:3]([NH2:24])=[O:2])=[CH:9][CH:10]=1)[C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1

Participants

3

Reactant 2

HCID 14923Ammonium HydroxideHCID 28638020HCID 28638020, compound

Product 1

HCID 9994024HCID 9994024, compoundYield 85%

Procedure

Prepared in analogy to example 3 from N-(4-benzyloxy-phenyl)-malonamic acid methyl ester and ammonium hydroxide. Yield=85%. Colorless solid. MS: m/e=285.1 (M++H).

Sources & evidence

ORD record
ord-fbbca94741174513aa7c822fc237ba8f
Source dataset
uspto-grants-2006_05
Patent number
US07053245B2

Reaction notes

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